MIL-DTL-700B
4.6.7 Rosin and rosin derivatives. The test for rosin and rosin
derivatives shall be in accordance with ASTM D 1542. A portion of the
separated nonvolatile vehicle shall be used for the test. Rosin and rosin
derivatives shall be as specified in 3.4.4.
4.6.8 Dilution stability. Dilution stability with thinner shall be
determined in accordance with method 4203.1 of FED-STD-141. Fifty milliliters
(mL) of enamel and 50 mL of paint thinner conforming to type I of A-A-2904
shall be used. Observations shall be made immediately after mixing and 30
minutes after mixing. Compatibility with thinner shall be as specified in
3.4.6.
4.6.9 Condition in container. A container of the product in the size
ordered shall be inspected. The product shall be equilibrated to test
laboratory conditions [nominal 23 C (73 F)]. Evidence of pressure or vacuum
in the unopened container shall be noted. The container shall then be opened
and examined in accordance with method 3011.1 of FED-STD-141 for evidence of
skinning, corrosion of container interior, odor of putrefaction, rancidity or
souring, gell bodies, and hard settling. If the sample is in a 1-liter (1-
quart) or smaller container, the character of the lower (or settled) layer
shall be determined with a spatula as specified in ASTM D 869. If the sample
is larger than 1 liter (1 quart), this step shall be omitted. The enamel
shall be hand-stirred 300 stirs in 2 minutes with a spatula appropriate to the
container, stirring so as to ensure uniform distribution of any settled
material. Immediately after stirring, the consistency of the enamel shall be
measured using the Krebs-Stormer viscometer. The enamel shall be applied to a
test panel and after it has dried the enamel film shall be examined for grains
0.8 mm (1/32 inch) in diameter, even larger gelatinous lumps, and streaks
caused by such grains or lumps. The condition of the product shall be as
specified in 3.4.5.
4.6.10
Storage stability.
4.6.10.1 Full container. Storage stability shall be tested in
accordance with ASTM D 1849. A container of the product of the size ordered
shall be stored at the temperature recommended in the manufacturer's data
sheet or ASTM F 718 for a period of 1 year. After completion of 1 year, the
stored sample shall be equilibrated to test laboratory conditions [nominal 23 C
(73 F)]. Evidence of pressure or vacuum in the unopened container shall be
noted. The container shall then be opened and examined in accordance with
method 3011.1 of FED-STD-141 for evidence of skinning, corrosion of container
interior, odor of putrefaction, rancidity, or souring. If the sample is in a
1-liter (1-quart) or smaller container, the character of the lower (or
settled) layer shall be determined with a spatula as specified in ASTM D 869.
If the sample is larger than 1 liter (1 quart), this step shall be omitted.
The enamel shall be hand-stirred 300 stirs in 2 minutes with a spatula
appropriate to the container, stirring so as to ensure uniform distribution of
any settled material. Immediately after stirring, the consistency of the
enamel shall be measured using the Krebs-Stormer viscometer. The enamel shall
be applied to a test panel and after it has dried the enamel film shall be
examined for grains 0.8 mm (1/32 inch) in diameter, even larger gelatinous
lumps, and streaks caused by such grains or lumps. The condition of the
product shall be as specified in 3.4.5.1.1.
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